Pyrolysis of perhydro[1,2-c][1,3]oxazines: a green method of synthesizing 2,3-dehydropiperidine enamines |
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| Authors: | A. Gilbert Cook Christine A. Schering Pauline A. Campbell Samantha S. Hayes |
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| Affiliation: | Department of Chemistry, Valparaiso University, Valparaiso, IN 46383, USA |
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| Abstract: | ![]()
Heat pyrolysis of the oxazines formed from 2-piperidineethanol produced 2,3-dehydropiperidine enamines. The same results were observed when these oxazines were irradiated with microwaves. Various 2-substituted perhydrooxazines were synthesized by allowing 2-piperidineethanol or 2-piperidinemethanol to react with aldehydes or ketones. |
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| Keywords: | Oxazines Pyrolysis Microwave Enamines Azomethine ylides |
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