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Synthesis and structure elucidation of three series of nitro‐2‐styrylchromones using 1D and 2D NMR spectroscopy
Authors:Ana I. R. N. A. Barros  Artur M. S. Silva
Affiliation:1. Chemistry Department, University of Trás‐os‐Montes e Alto Douro, 5001‐911 Vila Real, Portugal;2. Chemistry Department, University of Aveiro, 3810‐193 Aveiro, Portugal
Abstract:2‐Styrylchromones, although scarce in nature, constitute a group of oxygen heterocyclic compounds which have shown significant biological activities. New nitro‐2‐styrylchromones have been synthesised by the Baker–Venkataraman method, and the structure elucidation was accomplished using extensive 1D (1H, 13C) and 2D NMR spectroscopic studies (COSY, HSQC and HMBC experiments). Copyright © 2009 John Wiley & Sons, Ltd.
Keywords:1H NMR  13C NMR  HMBC  nitro‐2‐styrylchromones
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