| AgInS2纳米粒子的制备及其可见光催化活性 |
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| 引用本文： | 魏清莲,赵雪伶,姚平平,穆 劲. AgInS2纳米粒子的制备及其可见光催化活性[J]. 无机化学学报, 2011, 27(4): 692-696 |
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| 作者姓名： | 魏清莲 赵雪伶 姚平平 穆 劲 |
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| 作者单位： | 华东理工大学化学与分子工程学院,上海,200237 |
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| 摘 要： | 以水为溶剂,硫代乙酰胺为硫源,巯基乙酸为包覆剂,于低温下制备了正交相的AgInS2纳米粒子。用TEM、EDS和XRD对所制备的AgInS2纳米粒子的形貌、组成和晶相进行了表征。并考察了反应时间对AgInS2纳米粒子的晶相及其可见光催化降解活性的影响。结果表明:延长反应时间可以提高AgInS2纳米粒子的结晶性和可见光催化活性。
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| 关 键 词： | AgInS2纳米粒子 硫代乙酰胺 巯基乙酸 低温液相合成 可见光催化 |
Preparation and Visible Light Photocatalytic Activity of AgInS2 Nanoparticles |
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| WEI Qing-Lian,ZHAO Xue-Ling,YAO Ping-Ping and MU Jin. Preparation and Visible Light Photocatalytic Activity of AgInS2 Nanoparticles[J]. Chinese Journal of Inorganic Chemistry, 2011, 27(4): 692-696 |
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| Authors: | WEI Qing-Lian ZHAO Xue-Ling YAO Ping-Ping MU Jin |
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| Affiliation: | School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, China,School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, China,School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, China and School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, China |
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| Abstract: | AgInS2 nanoparticles with orthorhombic structure were prepared via a wet chemical route at low temperature using water as solvent, thioacetamide as sulfur source and mercaptoacetic acid as capping agent. The morphology and composition as well as crystal phase of AgInS2 nanoparticles were characterized by TEM, EDS and XRD. The effects of reaction time on the crystal phase and the visible light photocatalytic degradation activity of AgInS2 nanoparticles were also investigated. The results showed that the extention of preparation time could improve the crystallinity as well as the visible light photocatalytic activity of the particles. |
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| Keywords: | AgInS2 nanoparticles thioacetamide mercaptoacetic acid low temperature wet chemistry synthesis visible light photocatalysis |
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