| 微波辐射下8-溴腺苷及其衍生物的绿色合成 |
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| 引用本文： | 渠桂荣,张志广,郭海明,夏然,耿明伟. 微波辐射下8-溴腺苷及其衍生物的绿色合成[J]. 合成化学, 2007, 15(2): 195-197 |
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| 作者姓名： | 渠桂荣 张志广 郭海明 夏然 耿明伟 |
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| 作者单位： | 河南师范大学,化学与环境科学学院,河南,新乡,453007;河南师范大学,化学与环境科学学院,河南,新乡,453007;河南师范大学,化学与环境科学学院,河南,新乡,453007;河南师范大学,化学与环境科学学院,河南,新乡,453007;河南师范大学,化学与环境科学学院,河南,新乡,453007 |
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| 基金项目： | 国家自然科学基金资助项目(20372018) |
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| 摘 要： | 以Br2为溴化试剂,水为溶剂,微波辐射5 min,合成了6种8-溴腺苷衍生物,收率76%~85%,其结构经1HNMR,HR-MS和元素分析表征。
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| 关 键 词： | 腺苷 溴化 绿色溶剂 微波辐射 绿色合成 |
| 文章编号： | 1005-1511（2007）02-0195-03 |
| 收稿时间： | 2006-11-13 |
| 修稿时间： | 2006-11-13 |
Green Synthesis of 8-Bromoadenosine and Its Derivatives under Microwave Irradiation |
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| QU Gui-rong,ZHANG Zhi-guang,GUO Hai-ming,XIA Ran,GENG Ming-wei. Green Synthesis of 8-Bromoadenosine and Its Derivatives under Microwave Irradiation[J]. Chinese Journal of Synthetic Chemistry, 2007, 15(2): 195-197 |
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| Authors: | QU Gui-rong ZHANG Zhi-guang GUO Hai-ming XIA Ran GENG Ming-wei |
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| Affiliation: | College of Chemistry and Environmental Science, Henan Normal University, Xinxiang 453007, China |
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| Abstract: | Using Br2 as a bromination reagent and water as a solvent,8-bromoadenosine and its six derivatives were obtained in 76%~85% yields under microwave irradiation for 5 min.The structures were confirmed by 1H NMR,HR-MS and MS. |
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| Keywords: | adenosine bromination green solvent microwave irradiation green synthesis |
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