| 涂渍极性及强极性固定相硅膜改性弹性玻璃毛细管柱的研制 |
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| 引用本文： | 张桂琴,谢红卫.涂渍极性及强极性固定相硅膜改性弹性玻璃毛细管柱的研制[J].分析化学,1994,22(5):485-487. |
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| 作者姓名： | 张桂琴 谢红卫 |
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| 作者单位： | 中国科学院长春应用化学研究所!长春130022(张桂琴，谢红卫，马玉珍)，齐齐哈尔市天然气公司设计院(刘恒秋) |
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| 基金项目： | 国家自然科学基金资助项目 |
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| 摘 要： | 本文工作研究了极性、强极性固定液直接涂渍在硅膜改性弹性玻璃毛细管内壁上，经优化温度老化色谱柱，成功地研制出ＯＶ－２２５，ＤＥＧＳ，Ｓｉｌａｒ５，Ｓｉｌａｒ９，Ｓｉｌａｒ１０等硅膜改性弹性玻璃毛细管柱，各种柱子均具有柱效高，热稳定性好的色谱性能。
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| 关 键 词： | 硅膜 弹性玻璃 毛细管柱 改性 涂渍 |
Flexible Glass Capillary Column Modified by Silicon Film With Polar and Strong-polar Stationary Phase of Chromatography |
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| Zhang Guiqin,Xie Hongwei,Ma Yuzhen,Liu Hengqiu.Flexible Glass Capillary Column Modified by Silicon Film With Polar and Strong-polar Stationary Phase of Chromatography[J].Chinese Journal of Analytical Chemistry,1994,22(5):485-487. |
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| Authors: | Zhang Guiqin Xie Hongwei Ma Yuzhen Liu Hengqiu |
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| Abstract: | Polar and strong-polar stationary phases, OV-225, DECS, Silar 5,Silar 9, Silar 10, were directly coated on flexible glass capillary column modified by silicon film through electing suitable ageing temperature of column. The type of polar and strong-polar columns prepared posseses good chromatographic performance. Column efficiency, inertness and thermal stability of the columns were all nice. |
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| Keywords: | Silicon film Flexible glass capillary column Polar stationary Strong-polar stationary |
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