Synthesis of 2,3,4,5-tetranitropyrrole |
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Authors: | Jerald C. Hinshaw W. Wayne Edwards Clifford George Richard Gilardi |
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Abstract: | Dealkylation of 1-tert-butyl-2,3,4-trinitropyrrole in boiling trifluroacetic acid gave 2,3,4-trinitropyrrole, the structure of which was confirmed by X-ray crystallography. Treatment of this trinitropyrrole with nitric acid/oleum briefly at 60° gave 2,3,4,5-tetranitropyrrole. |
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