Abstract: | ![]() Antimony(III)-butoxo Compounds Tri(tert.-butoxo)stiban 1 reacts with antimony(III) chloride dependent from the molar ratio to yield Sb(OtBu)2Cl 2 and Sb4Cl7O(OtBu)3 3 resp ‥ 3 are discrete molecules with a cage structure. 2 is associated by oxygen bridges. The vibrational spectra of 1–3 are assigned. |