| 季戊四醇四乙酸酯的合成 |
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| 引用本文： | 俞善信,文瑞明,丁亮中. 季戊四醇四乙酸酯的合成[J]. 合成化学, 2001, 9(4): 365-367 |
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| 作者姓名： | 俞善信 文瑞明 丁亮中 |
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| 作者单位： | 益阳师范高等专科学校化学系,湖南,益阳,413049;益阳师范高等专科学校化学系,湖南,益阳,413049;益阳师范高等专科学校化学系,湖南,益阳,413049 |
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| 摘 要： | 比较了硫酸、一水硫酸氢钠、六水三氯化铁和十二水合硫酸铁铵在合成季戊四醇四乙酯酯中的催化活性。研究了硫酸氢钠催化合成季戊四醇四乙酯酯的反应条件,在优化反应条件下酯收率达88％,并通过熔点、元素分析和红外光谱进行表征。
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| 关 键 词： | 季戊四醇四乙酸酯 合成 硫酸氢钠 催化 |
| 文章编号： | 1005-1511(2001)04-365-03 |
| 修稿时间： | 2001-03-12 |
Synthesis of Pentaerythrityl Tetraacetate |
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| YU Shan xin,WEN Rui ming,DING Liang zhong. Synthesis of Pentaerythrityl Tetraacetate[J]. Chinese Journal of Synthetic Chemistry, 2001, 9(4): 365-367 |
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| Authors: | YU Shan xin WEN Rui ming DING Liang zhong |
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| Abstract: | The catalytic activities of sulfuric acid, sodium bisulfate monohydrate, ferric chlorie hexahydrate and ammonium ferric sulfate dodecahydrate in synthesis of pentaerythrityl tetraacetate are compared. The synthetic reaction conditions catalyzed by sodium bisulfate are studied. The yield can be up to 88% under the optimum condition and the product was characterized by melting point, elemental analysis and IR spectrum. |
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| Keywords: | pentaerythrityl tetracetate synthesis sodium bisulfate catalysis |
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