| 肉类食品中杂环胺检测的样品前处理及分析方法的研究进展 |
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| 引用本文： | 张仟春,肖小华,李攻科. 肉类食品中杂环胺检测的样品前处理及分析方法的研究进展[J]. 色谱, 2014, 32(9): 975-980. DOI: 10.3724/SP.J.1123.2014.05011 |
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| 作者姓名： | 张仟春 肖小华 李攻科 |
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| 作者单位： | 1. 中山大学化学与化学工程学院, 广东 广州 510275;2. 兴义民族师范学院生物与化学学院, 贵州 兴义 562400 |
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| 基金项目： | 国家自然科学基金项目，高等学校博士学科点专项基金项目，广东省自然科学基金项目 |
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| 摘 要： | 杂环胺是畜禽、鱼肉等食品在高温烹饪过程中生成的一类致癌、致突变化合物，高效、高选择性的样品前处理方法和高灵敏的分析方法是食品中痕量杂环胺分析检测的关键。本文综述了近年来溶剂萃取、固相萃取和固相微萃取等样品前处理方法，以及液相色谱、液相色谱-质谱等分析方法在食品中痕量杂环胺检测中的应用，结合现有研究对其发展趋势进行了展望。共引用文献51篇。
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| 关 键 词： | 分析方法 肉类食品 样品前处理 杂环胺 综述 |
| 收稿时间： | 2014-05-15 |
Advances on sample pretreatment and analytical method for the analysis of heterocyclic amines in meat products |
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| ZHANG Qianchun,XIAO Xiaohua,LI Gongke. Advances on sample pretreatment and analytical method for the analysis of heterocyclic amines in meat products[J]. Chinese journal of chromatography, 2014, 32(9): 975-980. DOI: 10.3724/SP.J.1123.2014.05011 |
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| Authors: | ZHANG Qianchun XIAO Xiaohua LI Gongke |
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| Affiliation: | 1. School of Chemistry and Chemical Engineering, Sun Yat-sen University, Guangzhou 510275, China;2. School of Biology and Chemistry, Xingyi Normal University for Nationalities, Xingyi 562400, China |
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| Abstract: | Heterocyclic amines (HAs) are considered as highly potential mutagens and carcinogens in cooked meat products. Efficient sample pretreatment as well as sensitive analytical method is very important for the determination of HAs in complex samples. In this paper, some sample pretreatment methods such as solvent extraction, solid-phase extraction, and solid-phase microextraction as well as analytical methods including liquid chromatography, and liquid chromatography-mass spectrometry are reviewed; The progress of HAs analysis is also prospected. A total of 51 references are cited. |
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| Keywords: | sample pretreatment analytical method heterocyclic amines meat products review |
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