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| Synthesis and Crystal Structure of the Derivative of β-elemene C_(20)H_(33)N·Cl_3CCOOH | |
| 引用本文： | GONG GuoLiang CHENG GuoBao HU JieHan DAI JianYing (Dalian Institute of Chemical Physics,the Chinese Academy of Sciences,Dalian 116023)= WU QiangJin (Fujian Institute of Research on the Structure of Matter,the Chinese Academy of Sciences,Fuzhou. Synthesis and Crystal Structure of the Derivative of β-elemene C_(20)H_(33)N·Cl_3CCOOH[J]. 结构化学, 1999, 0(4) |
| 作者姓名： | GONG GuoLiang CHENG GuoBao HU JieHan DAI JianYing (Dalian Institute of Chemical Physics the Chinese Academy of Sciences Dalian 116023)= WU QiangJin (Fujian Institute of Research on the Structure of Matter the Chinese Academy of Sciences Fuzhou |
| 作者单位： | GONG GuoLiang CHENG GuoBao HU JieHan DAI JianYing (Dalian Institute of Chemical Physics，the Chinese Academy of Sciences，Dalian 116023 |
| 摘 要： | １ＩＮＴＲＯＤＵＣＴＩＯＮβ ｅｌｅｍｅｎｅ，ａｓｅｓｑｕｉｔｅｒｐｅｎｏｉｄｃｏｍｐｏｕｎｄ，ｉｓａｎａｔｕｒａｌｐｒｏｄｕｃｔｉｓｏｌａｔｅｄｆｒｏｍｅｓｅｎ ｔｉａｌｏｉｌｃｏｎｔａｉｎｅｄｉｎｔｈｅｒｏｏｔａｎｄｓｔｅｍｏｆＣｈｉｎｅｓｅｈｅ... |
Synthesis and Crystal Structure of the Derivative of elemene C20H33NCl3CCOOH |
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| GONG GuoLiang CHENG GuoBao HU JieHan DAI JianYing. Synthesis and Crystal Structure of the Derivative of elemene C20H33NCl3CCOOH[J]. Chinese Journal of Structural Chemistry, 1999, 0(4) | |
| Authors: | GONG GuoLiang CHENG GuoBao HU JieHan DAI JianYing |
| Abstract: | The structure of the piperidine derivative of elemene C20H33NCl3CCOOH was determined by Xray crystallography. The crystal belongs to the orthorhombic system, space group P212121, a=12.303(4), b=22.064(7), c=9.002(4), V=2444(2)3, Z=4, Mr=450.88, Dc=1.23g/cm3, (MoK)=391cm-1, F(000)=960, Final R=0.050, Rw=0.067 for 2393 reflections I>3(I), GOF=1.91. The title compound is composed of trichloroacetate and the elemenyl piperidine cation. The latter contains two hexacyclic rings of elemene and piperidine, which adopt the chair conformations.= |
| Keywords: | elemene derivative crystal structure synthesis |
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