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PS-SNAP, a practical polymer-supported nitrosation reagent in organic synthesis |
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| Authors: | Didier Roche Claude Lardy Marc Prunier |
| Affiliation: | a Merck Serono, 4 Avenue du Président F. Mitterand, F91380 Chilly-Mazarin, France b Edelris, 115 Avenue Lacassagne, 69003 Lyon, France c Groupe Solabia, Route d’Oulins, 28260 Anet, France |
| Abstract: | PS-SNAP was designed and evaluated as a practical nitrosating polymer-supported reagent for the nitrosation of sec-amines. Nitrosated dialkyl amines, alkyl anilines, and bis-anilines were obtained in good yields and high purities after shaking the corresponding amines in the presence of an excess of the newly described reagent followed by simple filtration and removal of solvents. |
| Keywords: | N-Nitrosation Polymer-supported reagents boldFont" >PS-SNAP |
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