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Synthesis and X-ray Crystal Structure of a Methylene-bridged Glycoluril Dimer
Authors:SHE Neng-Fang  WU Yan-Dong  SUN Jing-Jing  WU An-Xin
Affiliation:Key Laboratory of Pesticide & Chemical Biology,Ministry of Education,College of Chemistry,Central China Normal University,Wuhan 430079,China
Abstract:
The synthesis and X-ray crystal structure of a methylene-bridged glycoluril dimer 2 was reported.The methylene-bridged glycoluril dimer 2(C_(38)H_(36)Br_4N_8O_(12),M_r=1116.35)crystalli96.263(1),γ=101.606(1)°,ν=4239.3(4)(A)~3,Z=4,D_c=1.749 g/cm~3,μ=3.869 mm~(-1) and F(000)=2224.It crystallizes in an S-shaped conformation that displays two ethoxycarbonyl groups on each face of the molecule.
Keywords:methylene-bridged glycoluril dimer  X-ray crystal structure  S-shape  
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