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A review of oxygen-17 solid-state NMR of organic materials--towards biological applications |
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| Authors: | Lemaître V Smith M E Watts A |
| Institution: | a Biomembrane Structure Unit, Department of Biochemistry, Oxford University, South Parks Road, Oxford OX1 3QU, UK b Nestec S.A., BioAnalytical Department, Vers-Chez-Les-Blanc, CH-1000, Lausanne 26, Switzerland c Department of Physics, University of Warwick, Coventry CV4 7AL, UK |
| Abstract: | 17O solid state NMR of organic materials is developing rapidly. This article provides a snapshot of the current state of development of this field. The NMR techniques and enrichment protocols that are driving this progress are outlined. The 17O parameters derived from solid-state NMR experiments are summarized and the structural sensitivity of the approach to effects such as hydrogen bonding highlighted. The prospects and challenges for 17O solid-state NMR of biomolecules are discussed. |
| Keywords: | Oxygen-17 Solid-state NMR MAS DOR DAS MQMAS Amino acids Organic molecules Peptide Hemeprotein Hydrogen-bond Biological applications Review |
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