| 三唑酮的气相色谱分析 |
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| 引用本文： | 牛淑妍,许良忠,张前前.三唑酮的气相色谱分析[J].理化检验(化学分册),2002,38(11):564-565. |
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| 作者姓名： | 牛淑妍 许良忠 张前前 |
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| 作者单位： | 1. 青岛科技大学应用化学系,青岛,266003
2. 青岛海洋大学化学化工学院,青岛,266003 |
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| 摘 要： | 研究了三唑酮的气相色谱分析条件 ,选择以 10 %SE 30为固定液 ,ChromosorbW (AW DMCS)载体填充的色谱柱 ,选择邻苯二甲酸二乙酯为内标 ,采用内标标准曲线法作为定量分析的方法 ,相对标准偏差 <0 .94 % ,线性相关系数为 0 .9990 4 ,加标回收率在 10 0 .1%～ 10 1.9%之间。方法简便 ,快捷 ,重复性好。
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| 关 键 词： | 分析 气相色谱 三唑酮 内标标准曲线法 杀菌剂 农药 工业生产 |
| 文章编号： | 1001-4020(2002)11-0564-02 |
| 修稿时间： | 2001年4月29日 |
GC ANALYSIS OF TRIAZOLONE |
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| NIU Shu yan,XU Liang zhong.GC ANALYSIS OF TRIAZOLONE[J].Physical Testing and Chemical Analysis Part B:Chemical Analgsis,2002,38(11):564-565. |
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| Authors: | NIU Shu yan XU Liang zhong |
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| Abstract: | Analytical conditions of GC analysis of triazolone were studied. The chromatographic column was packed with 10% SE 30/Chromosorb W(AW DMCS), and the hydrogen flame ionization detector was used. Dimethyl phthalate was used as internal standard in the quantitative determination. Testing on a sample containing 10 60% of triazolone, gave a RSD value of 0.94%. Recoveries obtained by the standard addition method were in the range of 100.1% to 101.9%. Based on the data of internal standard curve, the following linear regression equation was obtained, Y=1.05108X +0.03513. The correlative coefficient of this equation was found to be 0.99904. |
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| Keywords: | Gas chromatography Triazolone Internal standard curve method |
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