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| 邻二氮菲苯妥英合锰(Ⅱ)三元配合物的合成、结构与抗微生物活性研究 | |
| 引用本文： | 胡喜兰,许兴友,王大奇,许同桃,顾海星.邻二氮菲苯妥英合锰(Ⅱ)三元配合物的合成、结构与抗微生物活性研究[J].无机化学学报,2007,23(9):1675-1678. |
| 作者姓名： | 胡喜兰 许兴友 王大奇 许同桃 顾海星 |
| 作者单位： | 1. 淮海工学院化学工程系,连云港,222005 2. 聊城大学化学化工学院,聊城,252059 3. 连云港职业技术学院化工系,连云港,222006 |
| 基金项目： | 江苏省自然科学基金;江苏省重点实验室基金;淮海工学院校科研和教改项目 |
| 摘 要： | The title complex Mn(pht)2(phen)] (Hpht=5，5-diphenylimidazoline-2，4-dione， phen=1，10-phenanthroline) was synthesized and characterized by elemental analysis， IR and X-ray diffraction single-crystal structure analysis. The compound crystallizes in the monoclinic system， space group C2/c with a=2.631 5(16) nm， b=0.924 5(6) nm， c=1.550 8(10) nm， β=116.231(7)°; V=3.384(4) nm3，Mr=737.66， Z=4， F(000)=1 524， Dc=1.448 g·cm-3， μ=0.446 mm-1， the final R=0.069 9 and wR=0.195 3. The complex was valued for its antimicrobial activity against some bacteria in vitro. It was found to be active against the four test bacterial organisms. CCDC: 616309. |
| 关 键 词： | Mn(Ⅱ)配合物 苯妥英 邻二氮菲 晶体结构 抗微生物活性 |
| 文章编号： | 1001-4861（2007）09-1675-04 |
| 修稿时间： | 2007-05-28 |
Synthesis, Crystal Structure and Antimicrobiai Activity of a New Ternary Mixed Ligand Complex [Mn(pht)2(phen)] |
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| HU Xi-Lan,XU Xing-You,WANG Da-Qi,XU Tong-Tao and GU Hai-Xing.Synthesis, Crystal Structure and Antimicrobiai Activity of a New Ternary Mixed Ligand Complex [Mn(pht)2(phen)][J].Chinese Journal of Inorganic Chemistry,2007,23(9):1675-1678. | |
| Authors: | HU Xi-Lan XU Xing-You WANG Da-Qi XU Tong-Tao and GU Hai-Xing |
| Institution: | 1.Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang, Jiangsu 222005;2.College of Chemistry and Chemical Engineering, Liaocheng University, Liaocheng, Shandong 252059;3.Department of Chemical Engineering, Lianyungang Technical College, Lianyungang, Jiangsu 222006 |
| Abstract: | The title complex Mn(pht)2(phen)] (Hpht=5,5-diphenylimidazoline-2,4-dione, phen=1,10-phenanthroline)was synthesized and characterized by elemental analysis, IR and X-ray diffraction single-crystal structure analysis.The compound crystallizes in the monoclinic system, space group C2/c with a=2.631 5(16) nm, b=0.924 5(6) nm, c=1.550 8(10) nm, β=116.231(7)°;V=3.384(4) nm3, Mr=737.66, Z=4, F(000)= 1 524, Dc=1.448 g·cm-3,μ=0.446 mm-1,the final R=0.069 9 and wR=0. 195 3. The complex was valued for its antimicrobial activity against some bacteria in vitro. It was found to be active against the four test bacterial organisms. CCDC: 616309. |
| Keywords: | manganese complex 5 5-diphenylimidazoline-2 4-dione 1 10-phenanthroline crystal structure antimicrobial activity |
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