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Spectroscopic and thermal properties of FeHg(SCN)4
Authors:X.Q. Wang  D. Xu  X.Q. Hou  X.F. Cheng  D.R. Yuan
Affiliation:a State Key Laboratory of Crystal Materials, Institute of Crystal Materials, Shandong University, Jinan 250100, PR China
b Qingdao Institute of Architecture and Engineering, Qingdao 266033, PR China
c School of Materials Science, Jinan University, Jinan 250022, PR China
d College of Environmental Science and Engineering, Institute of Modern Analysis, Shandong University, Jinan 250100, PR China
Abstract:
The preparation and characterization of iron mercury thiocyanate, FeHg(SCN)4 (abbreviated as FMTC) are described. The spectroscopic properties were characterized by X-ray powder diffraction (XRPD), infrared, Raman and UV-Vis-NIR transmission spectra. The thermal stability and thermal decomposition of FMTC were investigated by means of thermogravimetric analysis (TGA) and differential thermal analysis (DTA). The intermediates and final products of the thermal decomposition were identified by X-ray powder diffraction at room temperature.
Keywords:Iron mercury thiocyanate   X-ray powder diffraction   Infrared spectroscopy   Raman spectroscopy   Transmission spectra   Thermal analysis
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