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Rapid internal bubble formation in a microwave heated polymer observed in real-time by X-ray scattering
Authors:JBA Mitchell  E JerbyY Shamir  Y MeirJL Le Garrec  M Sztucki
Institution:a IPR., U.M.R. No. 6251 du C.N.R.S., Université de Rennes I, 35042 Rennes, France
b Faculty of Engineering, Tel Aviv University, Ramat Aviv, 69978, Israel
c European Synchrotron Radiation Facility, BP-220, 38043 Grenoble, France
Abstract:A combined study of small-angle and wide-angle X-ray scattering (SAXS/WAXS) of the melting of a nylon-6 sample by localized microwave radiation has shown that this method can reveal the presence of bubbles forming and disappearing rapidly in real time in the interior of the sample due to its thermal decomposition.
Keywords:SAXS  WAXS  Melting  Polymer melting  Bubble formation
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