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Velocity and ejector-jet assisted differential pumping: Novel design stages for environmental SEM
Authors:Gerasimos D Danilatos
Institution:1. Quantum Beam Science Directorate, Tokai Research and Development Center, Japan Atomic Energy Agency, Tokai, Ibaraki 319-1195, Japan;2. Department of Chemistry, Princeton University, Princeton, NJ 08544, USA;1. Indian Space Research Organization Propulsion Complex, Mahendragiri, Tamil Nadu, India;2. Department of Mechanical Engineering, St. Xavier''s Catholic College of Engineering, Chunkankadai, Tamil Nadu, India;1. College of Chemical Engineering, Huaqiao University, Xiamen 361021, PR China;2. Department of Chemical and Materials Engineering, National I-Lan University, I-Lan 260, Taiwan;1. School of Ocean and Civil Engineering, Dalian Ocean University, Dalian 116023, China;2. School of Energy and Power Engineering, Dalian University of Technology, Dalian 116024, China
Abstract:Velocity and ejection pumping are proposed as novel evacuation techniques to assist the static differential pumping already in use in the environmental scanning electron microscope. The gas velocity (or momentum) that accompanies the supersonic jet stream formed through the first pressure limiting aperture is used to initially force the gas out of the system by placing the second pressure limiting aperture at an optimum position in the gaseous jet. By this method, the gaseous particle thickness between the two apertures is minimised and the required pumping speed of the first evacuation stage is also reduced to an absolute minimum. A further improvement is achieved by inserting an appropriately shaped baffle between the two apertures, which shields the second aperture from the gas jet of the first and acts as an ejector-jet pump. The gas leak rate through the second aperture is maintained at an acceptable low level by both systems, even below the static leak rate level when the ejector-jet design is used, in particular. The result of either method has a double benefit, namely, the electron beam loss in the intermediate pumping stage is minimised together with a reduction of pump speed requirements. This translates to best instrument performance and minimal manufacturing costs.
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