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检出限的涵义和计算方法
引用本文:王艳洁,那广水,王震,徐恒振,姚子伟.检出限的涵义和计算方法[J].化学分析计量,2012,21(5):85-88.
作者姓名:王艳洁  那广水  王震  徐恒振  姚子伟
作者单位:国家海洋局近岸海域生态环境重点实验室,国家海洋环境监测中心,大连116023
基金项目:海洋公益专项资助项目(201105013);国家海洋局近岸海域生态环境重点实验室开放基金(201110)
摘    要:介绍仪器检出限、方法检出限及样品检出限的基本定义及涵义,以气相色谱法测定海水中的十氯酮为例,进行不同方法的检出限计算,讨论了不同方法计算检出限引起的差异及计算方法中所选取参数的合理性,对如何科学使用检出限进行实验室质量控制提出了建议.

关 键 词:检出限  涵义  计算方法  区别

Connotation and Calculation Methods of Detection Limit
Wang Yanjie , Na Guangshui , Wang Zhen , Xu Hengzhen , Yao Ziwei.Connotation and Calculation Methods of Detection Limit[J].Chemical Analysis And Meterage,2012,21(5):85-88.
Authors:Wang Yanjie  Na Guangshui  Wang Zhen  Xu Hengzhen  Yao Ziwei
Institution:(Key Laboratory for Ecological Environment in Coastal Areas,National Marine Environmental Monitoring Center,Dalian 116023,China)
Abstract:The definition and connotation of the instrument detection limit,method detection limit and sample detection limit were introduced.Base on the determination of kepone in seawater by gas chromatography,several calculations methods were introduced about detection limit and the application.The difference of the calculating results and the rationality of selected parameter were discussed.A suggestion was given about how to use the detection limit to carry out the quality control in analysis laboratory scientifically.
Keywords:detection limit  connotation  calculation method  difference
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