| 金矿石中高含量锑的断续流动氢化物发生-原子荧光光谱法快速测定 |
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| 引用本文： | 祝建国,张涛,陈世焱,毛振才.金矿石中高含量锑的断续流动氢化物发生-原子荧光光谱法快速测定[J].分析测试技术与仪器,2009,15(3):173-175. |
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| 作者姓名： | 祝建国 张涛 陈世焱 毛振才 |
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| 作者单位： | 1. 国土资源部兰州矿产资源监督检测中心,甘肃,兰州,730050
2. 国土资源部兰州矿产资源监督检测中心,甘肃,兰州,730050 |
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| 摘 要： | 采用王水（1＋1）水浴分解样品,氢化物发生-原子荧光光谱法（HG-AFS）测定金矿石中高含量的锑.其方法回收率在95.0%-102.0%之间,相对标准偏差在1.0%-3.4%之间,方法检出限为3.0×10-10g/mL,经试验证实该方法可测范围宽、简便、快速、准确,实验室间对比分析结果吻合程度令人满意.
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| 关 键 词： | 金矿石 锑 原子荧光光谱法 |
Rapid Determination of High Content Sb in Gold Ore with Interrupted Flow by Hydride Generation-Atomic Fluorescence Spectrometry |
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| ZHU Jian-guo,ZHANG Tao,CHEN Shi-yan,MAO Zhen-cai.Rapid Determination of High Content Sb in Gold Ore with Interrupted Flow by Hydride Generation-Atomic Fluorescence Spectrometry[J].Analysis and Testing Technology and Instruments,2009,15(3):173-175. |
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| Authors: | ZHU Jian-guo ZHANG Tao CHEN Shi-yan MAO Zhen-cai |
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| Institution: | Lanzhou Center of Product Quality Supervision and Inspection of National Land and Natural Resources;Lanzhou 730050;China |
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| Abstract: | With aqua regia-water bath to decompose the sample,a method for the determination of high content Sb in gold ore by hydride generation-atomic fluorescence spectrometry（HG-AFS）is reported.The method recovery is 95.0%～102.0%,the relative standard deviation is 1.0%～3.4%,detection limit is 3.0×10-10 g/mL.Experiments rerified that the method has the adventages of wide measurement range,simplicity.rapidity and higher accuracy.The results of contrast analysis among laboratories are satifactory. |
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| Keywords: | gold ore Sb atomic fluorescence spectrometry |
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