| Abstract: | Introduction of a sample at a programmed temperature is an attractive approach both for dilute samples in large volumes and to prevent discrimination inside the syringe needle with this injection into a capillary gas Chromatograph. Quantitative data obtained with glass liners packed with trapping materials including glass wool, Tenax TA, Chromosorb 101 and Thermotrap-TA to analyze chlorinated and sulfur compounds are compared. To eliminate the solvent, these vapors were vented through the injection port cap, which provided greater efficiency than through the split line. |
