Size-controlled synthesis of SnO2 nanoparticles using reverse microemulsion method |
| |
| Institution: | 1. Department of Chemistry, Sciences & Arts Faculty, Sakarya University, 54187 Sakarya, Turkey;2. Department of Metallurgy and Material Engineering, Engineering Faculty, Sakarya University, 54187, Sakarya, Turkey;1. Chemistry of Heterocycles and Natural Product Research Laboratory, Organic Chemistry Division, School of Advanced Sciences, VIT University, Vellore 632 014, Tamilnadu, India;2. Physical Sensor Laboratory, MEMS and Sensor Division, School of Electronics Engineering, VIT University, Vellore 632 014, Tamilnadu, India;1. Inorganic Chemistry Department, National Research Centre, Dokki, Giza, 12622, Egypt;2. Chemistry Department, Faculty of Science, Ain Shams University, Cairo, 11566, Egypt;1. Institute of Nuclear Physics Polish Academy of Sciences, PL-31342 Krakow, Poland;2. Centre for Synthesis and Characterization of Nanomaterials, University of East Sarajevo, Faculty of Technology, Zvornik, Bosnia and Herzegovina |
| |
| Abstract: | Tin oxide nanoparticles were prepared using an ionic surfactant (sodium dodecyl sulfate) and tin (IV) chloride as an inorganic precursor via the reverse microemulsion method. The size of the nanoparticles is controlled by variation of water-to-surfactant ratio. Eliminating of surfactant in prepared nanoparticles was confirmed by the infrared spectroscopy after sequential calcinations. Transmission electron microscopy, surface area, pore volume, average pore diameter, pore size distribution and X-ray diffraction results were used for evaluation of size distribution, shape and structure of prepared SnO2 nanoparticles. Transmission electron micrographs confirmed that the obtained materials are spherical nanoparticles. The X-ray diffraction results show the crystalline phases of all samples are SnO2 with tetragonal structured crystal. In addition, the X-ray diffraction and transmission electron microscopy data showed that the size of SnO2 nanoparticles decreased with decreasing the water-to-surfactant ratio. |
| |
| Keywords: | Nanoparticles Tin oxide Microemulsion SDS |
| 本文献已被 ScienceDirect 等数据库收录！ |
|
