Structure of the Oxonium Compound of Pefloxacinium Hexachloridostannate(IV) |
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Authors: | A D Vasiliev N N Golovnev |
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Institution: | 1.Siberian Federal University,Krasnoyarsk,Russia;2.Kirensky Institute of Physics, Federal Research Center KSC, Siberian Branch,Russian Academy of Sciences,Krasnoyarsk,Russia |
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Abstract: | The structure of tris{hexachloridostannate(IV)}-hexachloride-tetrakis(pefloxacinium)-tetraoxonium undecahydrate (CCDC 1551760) 4PefH 3 2+ , 4H3O+, 3SnCl 6 2? , 6Cl?, 11H2O (I), (PefH is pefloxacin) is determined. The I crystals are triclinic: a = 13.5474(10) Å, b = 15.2859(11) Å, c = 15.6586(11) Å, α = 94.467(1)°, β = 105.477(1)°, γ = 111.560(1)°, V = 2849.9(4) Å3, space group Pī, Z = 1. The structure is stabilized by multiple intermolecular hydrogen bonds and π–π-interactions between the PefH32+ ions. |
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