Formation of a disordered layer lattice during the intercalation of water into anhydrous vanadyl phosphate |
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Authors: | Ludvík Bene? Vítězslav Zima |
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Institution: | (1) Joint Laboratory of Solid State Chemistry of the Academy of Sciences of the Czech Republic and University of Pardubice, Studentská 84, 530 09 Pardubice, Czech Republic |
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Abstract: | The course of intercalation of water into 1-VOPO4 has been studied by thermomechanical analysis and X-ray diffraction. Neither formation of vanadyl phosphate monohydrate nor staging were observed during the intercalation. The broadening and the shift of the positions of the lines in the diffractograms have been explained by the random stacking of intercalated and nonintercalated layers in the sample. |
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Keywords: | Intercalation X-ray powder diffraction vanadyl phosphate |
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