Intercalation of paramagnetic compounds in graphite fluoride with the composition C2Fx |
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Authors: | N F Yudanov E G Boguslavskii I I Yakovlev S P Gabudar |
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Institution: | 1. Academy of Sciences of the USSR, Novosibirsk
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Abstract: | 1. |
A method has been developed for the intercalation of solid substances from solutions in organic solvents into graphite fluoride C2Fx.
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Molecules of inserted paramagnetic copper complexes and nitroxyl radicals assume oriented positions between the structural layers in graphite fluoride.
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The planes of molecules of bis-chelate Cu(II) complexes with acetylacetone, o-hydroxyquinoline, and phenylsalicylaldimine were determined to lie parallel to the C2Fx planes.
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A method has also been suggested for the preparation of samples from C2Fx·yA compounds with a higher degree of texturizing (more nearly complete orientation) than can be achieved by pelletizing.
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 272–276, February, 1988. |
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