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Solid state analysis in mechanochemistry by high resolution 27Al solid state NMR spectroscopy |
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| Authors: | Werner Storek Hendrik Kosslick Vu Anh Tuan Hans-Peter Hennig |
| Affiliation: | 1. Federal Institute for Materials Research and Testing, Rudower Chaussee 5, D-12489, Berlin, Germany 2. Centre of Heterogeneous Catalysis, Rudower Chaussee 5, D-12489, Berlin, Germany 3. WITEGA-Research GmbH, Rudower Chaussee 5, D-12489, Berlin, Germany |
| Abstract: | Modern solid state NMR techniques [one-dimensional magic angle spinning (MAS) and two-dimensional quadrupole nutation experiments with MAS] are applied for the characterization of mechanochemically activated inorganic powders such as hydrargillite [γ-Al(OH)3] and pseudo-boehmite [synthetic γ-AlO(OH)]. The materials were activated in a vibration mill. |
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