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| CRYSTAL STRUCTURE OF ORGANOMETALLIC COMPLEX [Zn（pom）2Br2] | |
| 引用本文： | 李宋贤,王哲民,等. CRYSTAL STRUCTURE OF ORGANOMETALLIC COMPLEX [Zn（pom）2Br2][J]. 结构化学, 1993, 12(1): 35-37 |
| 作者姓名： | 李宋贤 王哲民 等 |
| 摘 要： | <正> Organometallic complex [Zn (pom)2Br2] (pom = 3-M ethyl-4-Ni-tropyridine-1-Oxide), C12H12Br2N4O6Zn, MT = 533. 44, triclinic, P1, a = 11. 450 (3), b = 13. 027(2), c=6. 605(1)A, α=101. 25(1),β=96. 96(2), γ=108. 06 (2)°,V = 901.2(4)A3, Z = 2, Dc=1. 97 gcm-3,λ(MoKa) = 0. 71069A , F(OOO) = 520, μ= 58. 21cm-1, final R = 0. 040 for 2192 observed reflections, T = 296K. The compound is a mononuclear complex, containing a tetrahedrally coordinated zinc atom. |
| 关 键 词： | 晶体结构 有机金属配合物 溴化锌 3－甲基－4－硝基氧化吡啶 |
CRYSTAL STRUCTURE OF ORGANOMETALLIC COMPLEX [Zn(pom)_2Br_2] |
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| Affiliation: | [1]DepartmentofChemistry,FuzhouUniversity,Fuzhou,3500 [2]DepartmentofChemistry,FuzhouU |
| Abstract: | Organometallic complex [Zn (pom)2Br2] (pom = 3-M ethyl-4-Ni-tropyridine-1-Oxide), C12H12Br2N4O6Zn, MT = 533. 44, triclinic, P1, a = 11. 450 (3), b = 13. 027(2), c=6. 605(1)A, α=101. 25(1),β=96. 96(2), γ=108. 06 (2)°,V = 901.2(4)A3, Z = 2, Dc=1. 97 gcm-3,λ(MoKa) = 0. 71069A , F(OOO) = 520, μ= 58. 21cm-1, final R = 0. 040 for 2192 observed reflections, T = 296K. The compound is a mononuclear complex, containing a tetrahedrally coordinated zinc atom. |
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