| 化合物(Et4N)2[Pd2(mp)2(μ-mpH)2]的NMR研究 |
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| 引用本文： | 吴达旭,施继成.化合物(Et4N)2[Pd2(mp)2(μ-mpH)2]的NMR研究[J].波谱学杂志,1996,13(4):377-381. |
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| 作者姓名： | 吴达旭 施继成 |
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| 作者单位： | 中国科学院福建物质结构研究所结构化学国家重点实验室, 福州 350002 |
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| 摘 要： | 采用1H-1H COSY,HMQC、HMBC等2D NMR技术对化合物(Et4N)2Pd2(mp)2(μ-mpH)2]进行1H、13C NMR谱数据分析与归属,表明它在DMSO溶液中仍保持原有固体状态的分子结构.
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| 关 键 词： | 化合物[Et4N)[Pd2(mp)2(μ-mpH)2] 邻巯基苯酚 同核质子相关谱 异核多量子相干相关谱 异核多键相关谱 |
| 收稿时间： | 1995-11-06 |
NMR STUDIES ON THE COMPOUND(Et4N)2[Pd2(mp)2(μ-mph)2] |
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| Wu Daxu,Shi Jicheng,Kang Beisheng.NMR STUDIES ON THE COMPOUND(Et4N)2[Pd2(mp)2(μ-mph)2][J].Chinese Journal of Magnetic Resonance,1996,13(4):377-381. |
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| Authors: | Wu Daxu Shi Jicheng Kang Beisheng |
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| Institution: | Stat Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou 350002 |
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| Abstract: | In this paper simulated proton spectrum and Homo-COSY,Hetero-CHCOR 2D NMR techniques were used to analyze and assign the 1H and 13C NMR spectra of the Compound (E4N)2Pd2(mp)2(μ-mph)2].The results indicate that the Compound isstable in DMSO solution as their molecular structures remain the same as those in the solid state. |
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| Keywords: | Compound (Et4N)2[Pd2(mp)2(μ-mph)]2 o-mercaptophenol 1H-1H COSY HMQC HMBC |
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