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微波溶剂热法合成纳米晶Cu2SnSe4及其结构研究
引用本文:刘兴芝,陈林,房大维,赵昌明,李俊,臧树良. 微波溶剂热法合成纳米晶Cu2SnSe4及其结构研究[J]. 无机化学学报, 2005, 21(6): 945-948
作者姓名:刘兴芝  陈林  房大维  赵昌明  李俊  臧树良
作者单位:辽宁大学化学科学与工程学院,沈阳,110036
基金项目:辽宁省教育厅科研基金资助项目(No.202102017)。
摘    要:The nanocrystal Cu2SnSe4 was synthesized by the microwave solvothermal technique and characterized by X-ray powder diffraction (XRD), transmission electron microscope (TEM) and X-ray photoelectron spectroscopy (XPS). Results show that the technique is fast, simple and energy saving, and the average size of the product is 20~30 nm. Optical absorption spectrum of Cu2SnSe4 shows that product with a band gap of 2.36 eV is a better semiconductor.

关 键 词:微波溶剂热; 纳米晶; 金属硒化物
文章编号:1001-4861(2005)06-0945-04
收稿时间:2004-11-15
修稿时间:2004-12-31

Synthesis and Properities of Nanocrystal Copper Tin Seleride by Microwave Solvothermal Technique
LIU Xing-Zhi,CHEN Lin,FANG Dai-Wei,ZHAO Cang-Ming,LI Jun and ZANG Shu-Liang. Synthesis and Properities of Nanocrystal Copper Tin Seleride by Microwave Solvothermal Technique[J]. Chinese Journal of Inorganic Chemistry, 2005, 21(6): 945-948
Authors:LIU Xing-Zhi  CHEN Lin  FANG Dai-Wei  ZHAO Cang-Ming  LI Jun  ZANG Shu-Liang
Affiliation:Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036,Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036,Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036,Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036,Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036 and Institute of Chemistry Science & Engineering, Liaoning University, Shenyang 110036
Abstract:The nanocrystal Cu2SnSe4 was synthesized by the microwave solvothermal technique and characterized by X-ray powder diffraction (XRD), transmission electron microscope (TEM) and X-ray photoelectron spectroscopy (XPS). Results show that the technique is fast, simple and energy saving, and the average size of the product is 20~30 nm. Optical absorption spectrum of Cu2SnSe4 shows that product with a band gap of 2.36 eV is a better semiconductor.
Keywords:solvothermal   nanocrystal   metal selenide
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