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X-ray crystal structure oftrans-dichlorobis(2,6-lutidine)palladium(II)
Authors:Pierre Losier  Donald C. MacQuarrie  Michael J. Zaworotko
Affiliation:(1) Department of Chemistry, Saint Mary's University, B3H 3C3 Halifax, Nova Scotia, Canada
Abstract:The X-ray structure oftrans-(2,6-lutidine)2PdCl2 has been determined. Golden orange crystals of the complex crystallize in the triclinic space group
$$Pbar 1$$
, with cell dimensionsa=7.6950(8),b=7.9705(10),c=8.0485(8)Å, agr=116.967(9), beta=113.343(8), and gamma=93.836(9)°;V=385.18(7)Å3 andZ=2. 1336 unique reflections withInet>3sgr (I) on refinement afforded values ofR=0.018 andRw=0.023.
Keywords:2,6-Lutidine complex  palladium(II)  X-ray structure
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