Efficient copper-catalyzed coupling of aryl iodides and thiobenzoic acid |
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| Authors: | Naotaka Sawada Takahiro Itoh |
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| Institution: | a Process Research, Banyu Pharmaceutical Co. Ltd., 9-1, Kamimutsuna 3-Chome, Okazaki, Aichi 444-0858, Japan
b Merck Research Laboratories, Department of Process Research, PO Box 2000, Rahway, NJ 07065, USA |
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| Abstract: | A highly efficient copper-catalyzed coupling reaction of aryl iodides and thiobenzoic acid, using 10 mol % of copper iodide, 20 mol % of 1,10-phenanthroline, and iPr2NEt in toluene, was developed. This methodology is applicable to a variety of aryl iodides. |
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