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溶胶-凝胶法制备耐磨宽带SiO2/TiO2增透膜
引用本文:贾巧英,乐月琴,唐永兴,姜中宏.溶胶-凝胶法制备耐磨宽带SiO2/TiO2增透膜[J].光学学报,2004,24(1):5-69.
作者姓名:贾巧英  乐月琴  唐永兴  姜中宏
作者单位:中科院上海光学精密机械研究所高功率激光物理国家实验室,上海201800
基金项目:国家高技术 86 3 80 4 2资助课题
摘    要:以钛酸正丁酯Ti(OBu)4]、正硅酸乙酯(TEOS)为原料,采用溶胶—凝胶(sol—gel)提拉方法在K9光学玻璃基片上镀制得高透过的λ/4~λ/2型宽带增透膜。该增透膜的表面均匀性良好,均方根粗糙度(RMS)为1.201,平均粗糙度(RA)为0.934,具有一定的耐擦除性。经200℃热处理,膜层中的OH吸收峰已基本消失,在400~700nm光谱范围的透过率比基片的平均透过率提高6.6%。为实现大面积涂覆“神光”装置主放大器的防爆隔板玻璃,大幅度提高主放大器的抽运效率奠定基础。

关 键 词:溶胶-凝胶法  二氧化硅  二氧化钛  薄膜物理学  宽带增透膜  均方根粗糙度  热处理  透过率  抽运效率
收稿时间:2002/10/18

Broadband and Scratch-Resistant Antireflective Coating Composed of SiO2/TiO2 Prepared from Sol-Gel Processing
Jia Qiaoying Le Yueqin Tang Yongxing Jiang Zhonghong.Broadband and Scratch-Resistant Antireflective Coating Composed of SiO2/TiO2 Prepared from Sol-Gel Processing[J].Acta Optica Sinica,2004,24(1):5-69.
Authors:Jia Qiaoying Le Yueqin Tang Yongxing Jiang Zhonghong
Abstract:type of λ/4~λ/2 broadband antireflective coating has been developed by sol-gel dipping method with tetrabutylorthotitanate and tetraethoxysilane (TEOS) as precursors. This antireflective coating possesses smooth and even surface,its average roughness is estimated having the value of RMS (1.201) and RA (0.934),and the specific scratch-resistant is good. Most -OH groups are eliminated at the temperature near 200 ℃. The average transmission of both-coated K9 substrate is increased 6.6% higher than uncoated one in the spectra from 400 nm to 700 nm. The antireflective coating is expected to coat amplifier blastshields of "Sheng-Guang: facility for enhancing the pumping efficiency of amplifiers
Keywords:film physics  sol-gel  broadband antireflective coatings  even surface  scratch-resistant
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