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Thermal decomposition and indirect structural determination of rare earth element picrates with the dtso ligand |
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| Authors: | P. Miranda Jr. J. Zukerman-Schpector J. R. Matos M. F. Máduar E. M. Aricó M. Linardi L. B. Zinner G. Vicentini |
| Affiliation: | (1) Departamento de Química, UFSC, Săo Carlos, SP -, Brazil E-mail;(2) Instituto de Química, USP, Săo Paulo, SP -, Brazil;(3) Instituto de Pesquisas Energéticas e Nucleares, Săo Paulo, SP -, Brazil |
| Abstract: | The complexes [Ln(pic)3(DTSO)3] (Ln=La, Lu and Y; pic=picrate; DTSO=1,3-dithiane-1-oxide) were synthesized and characterized. Indirect structural determination by far infrared spectroscopy is presented. Results from thermal decomposition of these complexes by TG/DTG and DSC techniques are reported. This revised version was published online in August 2006 with corrections to the Cover Date. |
| Keywords: | DSC TG/DTG far infrared spectroscopy lanthanide |
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