Thermal decomposition and indirect structural determination of rare earth element picrates with the dtso ligand |
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| Authors: | P Miranda Jr J Zukerman-Schpector J R Matos M F Máduar E M Aricó M Linardi L B Zinner G Vicentini |
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| Institution: | (1) Departamento de Química, UFSC, Săo Carlos, SP -, Brazil E-mail;(2) Instituto de Química, USP, Săo Paulo, SP -, Brazil;(3) Instituto de Pesquisas Energéticas e Nucleares, Săo Paulo, SP -, Brazil |
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| Abstract: | The complexes Ln(pic)3(DTSO)3] (Ln=La, Lu and Y; pic=picrate; DTSO=1,3-dithiane-1-oxide) were synthesized and characterized. Indirect structural determination by far infrared
spectroscopy is presented. Results from thermal decomposition of these complexes by TG/DTG and DSC techniques are reported.
This revised version was published online in August 2006 with corrections to the Cover Date. |
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| Keywords: | DSC TG/DTG far infrared spectroscopy lanthanide |
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