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离子色谱法测定饲料添加剂磷酸二氢钠中4种无机阴离子
引用本文:王珊珊,张锦梅,孙健. 离子色谱法测定饲料添加剂磷酸二氢钠中4种无机阴离子[J]. 中国无机分析化学, 2012, 2(3): 40-42
作者姓名:王珊珊  张锦梅  孙健
作者单位:青岛盛瀚色谱技术有限公司,山东 青岛 266101;青岛盛瀚色谱技术有限公司,山东 青岛 266101;山东省高青县计量所,山东 淄博 256300
基金项目:科技部科技型中小企业技术创新基金(09C26213711749)
摘    要:应用抑制电导检测离子色谱法建立了准确快速测定磷酸二氢钠中无机阴离子含量的分析方法。样品经过简单溶解后即可上机分析,分析时间小于30min。实验结果表明,方法的重现性好、灵敏度高、操作简便易行,还可以推广应用到其他工业原料如磷酸钠、磷酸氢钙及磷酸等的测定。

关 键 词:离子色谱法  磷酸二氢钠  无机阴离子
收稿时间:2012-07-02
修稿时间:2012-07-31

Determination of Four Inorganic Anions in Sodium Dihydrogen Phosphate as Feed Additive by Ion Chromatography
WANG Shanshan,ZHANG Jinmei and SUN Jian. Determination of Four Inorganic Anions in Sodium Dihydrogen Phosphate as Feed Additive by Ion Chromatography[J]. Chinese Journal of Inorganic Analytical Chemistry, 2012, 2(3): 40-42
Authors:WANG Shanshan  ZHANG Jinmei  SUN Jian
Affiliation:Qingdao Shenghan Chromatography Tech. Co. Ltd., Qingdao, Shandong 266101,China;Qingdao Shenghan Chromatography Tech. Co. Ltd., Qingdao, Shandong 266101,China;Institute of Metrology of Gaoqing in Shandong Province, Zibo, Shandong 256300,China
Abstract:A rapid and accurate method for determination of F-, Cl-, SO42-, NO3- in sodium dihydrogen phosphate by ion chromatography with suppressed conductivity detection was established.After simple dissolution treatment, the samples can be analyzed directly by the chromatography instrument with an analysis time of less than 30 minutes.The experimental results showed that the method had good reproducibility, high sensitivity and simplicity and can be applied for determination of other industrial raw materials, such as sodium phosphate, calcium hydrogen phosphate, phosphoric acid, and so on.
Keywords:ion chromatography  sodium dihydrogen phosphate  inorganic anions
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