A new electrochemical procedure for preparing 2,4,6-triphenylselenopyran from 1,5-diketones under conditions of acid catalysis |
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| Authors: | T. G. Dmitrienko S. S. Popova |
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| Affiliation: | (1) Technological Institute, Saratov State Technical University, Engels, Saratov oblast, Russia;(2) Saratov Military Institute of Chemical, Biological, and Radiation Protection, Saratov, Russia |
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| Abstract: | A new electrochemical procedure was developed for preparing 2,4,6-triphenylselenopyran from 1,5-diketones under conditions of acid catalysis at oxidative electrochemical activation of hydrogen selenide in the presence of a one-electron oxidizing agent in a nonaqueous solution. The electrolysis products were analyzed by gas chromatography with a mass-selective detector. |
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