Structure elucidation of an unexpected product from dehydration of a beta-hydroxyketone |
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| Authors: | Minter David E Winslow Christopher D Watson William H Bodige Satish |
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| Institution: | Department of Chemistry, Texas Christian University, Fort Worth, Texas 76129, USA. d.minter@tcu.edu |
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| Abstract: | The structure of an unexpected compound from the dehydration of an aldol addition product has been determined using 1-D and 2-D NMR techniques. This reaction is the last step in a new synthetic approach to the galanthan ring system. Complete 1H and 13C NMR assignments for two synthetic precursors are also reported. |
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| Keywords: | NMR 1H NMR 13C NMR HMQC HMBC de Mayo reaction galanthan nucleus |
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