| AFS-230E双道原子荧光光度计测定蔬菜中的砷和汞 |
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| 引用本文： | 张世仙.AFS-230E双道原子荧光光度计测定蔬菜中的砷和汞[J].中国无机分析化学,2015,5(1). |
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| 作者姓名： | 张世仙 |
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| 作者单位： | 遵义师范学院 化学化工学院 |
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| 基金项目： | 贵州省科技厅资助（黔科合J字LKZS[2012]28号）和遵义师范学院红色文化资源开发与区域经济研究中心资助（ZE2012009）。 |
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| 摘 要： | 采用湿法消解蔬菜样品，用AFS-230E型双道原子荧光光度计测定蔬菜中的As、Hg重金属含量。在最佳实验条件下，As、Hg元素的工作曲线相关系数(r)分别为0.9992、0.9996，检出限分别为0.0119ug/L、0.0139ug/L，回收率分别为：91.6%~101.50%，89.8%~97.3%，相对标准偏差（RSD%，n=7）分别为1.39%、0.52%，该法可供各地测定该类蔬菜中As、Hg等重金属元素含量的参考。
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| 关 键 词： | 湿法消解 AFS-230E型双道原子荧光光度计 蔬菜 砷 汞 |
Determination of arsenic and mercury in vegetables by AFS-230E double channel atomic fluorescence photometer |
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| ZHANG SHi-xian.Determination of arsenic and mercury in vegetables by AFS-230E double channel atomic fluorescence photometer[J].Chinese Journal of Inorganic Analytical Chemistry,2015,5(1). |
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| Authors: | ZHANG SHi-xian |
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| Institution: | Department of Chemisty ,Zunyi Normal College |
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| Abstract: | Using the wet digestion of vegetable samples, determination of the contents of As, Hg of heavy metals in vegetables by AFS-230E double channel atomic fluorescence photometer. Under the optimum experimental conditions, the correlation coefficient curve As, Hg elements (R) were 0.9992, 0.9996, the detection limits were 0.0119ug/L, 0.0139ug/L, recovery rates were: 91.6%~101.50%, 89.8%~97.3%, the relative standard deviation (RSD%, n=7) were 1.39%, 0.52%, the method for determination of the content of heavy metal element around As, Hg and so on the vegetables in the reference |
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| Keywords: | wet digestion AFS-230E double channel atomic fluorescence spectrometer vegetables arsenic mercury |
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