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TiC-MgO composite: an X-ray transparent and machinable heating element in a multi-anvil high pressure apparatus |
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| Authors: | Fang Xu Longjian Xie Akira Yoneda Nicolas Guignot Andrew King Guillaume Morard |
| Institution: | 1. Institut de Minéralogie, de Physique des Matériaux, et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Muséum National d’Histoire Naturelle, IRD Unité 206, Paris, Francefang.xu@upmc.fr![ORCID Icon]({"type":"image","src":"/templates/jsp/images/orcid.png"} "ORCID Icon") https://orcid.org/0000-0002-9537-662X;3. Institute for Planetary Materials, Okayama University, Misasa, Tottori, Japan;4. Synchrotron SOLEIL, L’Orme des Merisiers, Gif-sur-Yvette, France;5. Institut de Minéralogie, de Physique des Matériaux, et de Cosmochimie (IMPMC), Sorbonne Université, UMR CNRS 7590, Muséum National d’Histoire Naturelle, IRD Unité 206, Paris, France |
| Abstract: | ABSTRACTTiC-MgO composite was developed as a heating element for X-ray study in the multi-anvil high pressure apparatus. We synthesized TiC-MgO blocks (50–70 wt.% of TiC) by compression in a cold isostatic press followed by baking in a gas flow furnace. Heaters of tubular shape were manufactured from the synthesized blocks either by lathe or numerically controlled milling machine. The so-produced heating elements have been proved to generate temperatures up to 2250?K at 10?GPa, condition where classical graphite heaters are not suitable anymore due to graphite-diamond transition. These new heaters have been successfully used for in situ X-ray radiography and diffraction measurements on liquid Fe alloys, exploiting excellent X-ray transparency. |
| Keywords: | Multi-anvil heater TiC-MgO composite X-ray transparency high temperature |