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Thermal and magnetic behavior of Angustifolia Kunth bamboo fibers covered with Fe3O4 particles
Authors:S Calvo  NP Arias  O Giraldo  A Rosales-Rivera  O Moscoso
Institution:1. Laboratorio de Magnetismo y Materiales Avanzados, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales, Colombia;2. Laboratorio de Materiales Nanoestructurados y Funcionales, Facultad de Ciencias Exactas y Naturales, Universidad Nacional de Colombia, Sede Manizales, Manizales, Colombia;3. Departamento de Ingeniería Eléctrica, Electrónica y Computación, Facultad de Ingeniería y Arquitectura, Universidad Nacional de Colombia, Sede Manizales, Manizales, Colombia
Abstract:Several Angustifolia Kunth bamboo fibers, which have been previously treated with an alkaline solution, were coated with magnetite particles. The coating of the fibers was achieved by an in-situ co-precipitation method with Fe2+ and Fe3+in NaOH or NH4OH. The fibers were evaluated by chemical analysis using atomic absorption (A.A.) technique, structural characterization by X-ray diffraction (XRD), thermal stability with thermo-gravimetric analysis (TGA) in nitrogen at temperature range between 23 °C and 800 °C and magnetic behavior using vibrating sample magnetometry (VSM) applying a magnetic field between −27 KOe and 27 KOe at room temperature. We found that the thermal stability and magnetization depend of the synthesis method used to cover the Angustifolia Kunth bamboo fibers. In addition, an improved magnetic response was observed when NaOH solution is used to generate the magnetite coating on the fiber surface.
Keywords:Magnetite type materials  Superparamagnetism
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