Synthesis and crystalline and molecular structures of the morpholinylamide of N(R)-l-ephedrinylacetic acid |
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Authors: | K. M. Turdybekov A. B. Shalbaeva O. A. Nurkenov A. V. Kanakhin I. V. Kulakov A. M. Gazaliev |
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Affiliation: | (1) Institute of Phytochemistry, National Academy of Sciences of the Republic of Kazakhstan, Karaganda;(2) Institute of Organic Synthesis and Coal Chemistry, National Academy of Sciences of the Republic of Kazakhstan, Karaganda |
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Abstract: | The synthesis of the morpholinylamide of N(R)-1-ephedrinylacetic acid has been achieved by the interaction of (5S,6R)-4,5-dimethyl-6-phenylmorpholin-2-one with morpholine, and its structure has been shown by IR and PMR spectroscopies and x-ray structural analysis.Translated from Khimiya Prirodnykh Soedinenii, No. 1, pp. 108–112, January–February, 1999. |
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