Synthesis and characterization of 5-bromo-3-sec-butyl-6-methyluracil |
| |
| Authors: | Huixue Ren Yanzhao Yang Jimao Lin Yinshan Qi Yeqing Zhang |
| |
| Institution: | (1) School of Environmental Engineering, Shangdong Jianzhu University, Jinan, 250010, China;(2) School of Chemistry and Chemical Engineering, Shandong University, Jinan, 250001, China;(3) ZiBo HuaLian Mining Industry CO., LTD, Zibo, 256100, China |
| |
| Abstract: | A new synthetic method for 5-bromo-3-sec-butyl-6-methyluracil (Bromacil) using 2-bromobutane and urea as starting materials is described. The synthesis involved condensation,
cyclization and bromination with a total yield of 60%. The structure of Bromacil was determined by 1H NMR, 13C NMR and IR spectroscopy.
__________
Translated from Journal of Shandong University (Natural Science Edition), 2007, 42(7): 9–12 译自: 山东大学学报(自然科学版)] |
| |
| Keywords: | Bromacil condensation cyclization bromination |
| 本文献已被 万方数据 SpringerLink 等数据库收录！ |
|
