| A Novel Fused Phosphorus Heterocycle：4—（1′，2′,3′,4′—Tetrahydro—1,3,2—benzodiaaphosphorin—2′—sulfide）—3,4b,4a—thiazphosphaphenanthridine Derivative |
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| 引用本文： | JunMinHUANG HuiCHEN 等.A Novel Fused Phosphorus Heterocycle：4—（1′，2′,3′,4′—Tetrahydro—1,3,2—benzodiaaphosphorin—2′—sulfide）—3,4b,4a—thiazphosphaphenanthridine Derivative[J].中国化学快报,2002,13(2):125-128. |
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| 作者姓名： | JunMinHUANG HuiCHEN |
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| 作者单位： | [1]InstituteofElemento－OrganicChemistry,NationalLaboratoryofElemento－OrganicChemistry,NankaiUniversity,Tianjin300071 [2]InstituteofElemento－OrganicChemistry,NationalLaboratoryofElemento－OrganicChemistry,Nan |
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| 摘 要： | The first example of fused phosphorus heterocyclic 4-1′-(β-bromoethyl)-4′-oxo-3′-propyl-1′,2′,3′,4′-tetrahydro-1,3,2-benzodiazaphosphorin-2′-sulfide]-1,2,3,4,4a,4b,5,6-octahydro-6-oxo-5-propyl-3,4b,4a-thiazphosphaphenanthridine 4a,2′-dioxide was synthesized in excellent yield by refluxing a mixture of 1-(2-bromoethyl)-2,3-dihydro-3-propyl-1,3,2-benzodiazaphos phorin-4(1H)-one 2-oxide with carbon disulfide in benzene in the presence of triethylamine.
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| 关 键 词： | 4－（1′，2′ 3′ 4′－四氢化－1，3，2－苯并二氮杂磷－2′－硫醚）－3，4b 4a－硫代氮杂磷杂菲啶 衍生物 熔融磷杂环 |
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