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YBCO涂层导体用YSZ缓冲层的快速制备研究
引用本文:冯啸,熊杰,张飞,夏钰东,赵晓辉,陶伯万. YBCO涂层导体用YSZ缓冲层的快速制备研究[J]. 低温与超导, 2012, 2(2): 19-23,33. DOI: 10.3969/j.issn.1001-7100.2012.02.005
作者姓名:冯啸  熊杰  张飞  夏钰东  赵晓辉  陶伯万
作者单位:1.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054;2.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054;3.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054;4.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054;5.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054;6.电子科技大学电子薄膜与集成器件国家重点实验室,成都60054
摘    要:基于反应直流溅射法,采用镶嵌有钇粒的金属锆作为靶材,去离子水蒸汽为氧化反应气体,在有Y2O3种子层的双轴织构Ni -5at.%W基带上,系统地研究了温度和卷绕速度对YSZ阻挡层薄膜结构及表面形貌的影响.X射线衍射(XRD)分析表明,生长温度在700℃时制备的薄膜呈现明显的(002)取向;原子力显微镜(AFM)分析显示,该温度下制备的薄膜表面致密、无孔洞、无裂纹.在不同的卷绕速度下,虽然薄膜均为纯c轴取向,但其均方根粗糙度(RMS)和微粒大小均有较大差别.快速制备可达到抑制基片表面氧化、助于薄膜取向改善、提高薄膜制备效率的目的.

关 键 词:反应直流溅射  YSZ阻挡层  快速制备  生长温度  卷绕速度

The influences of rapid growth of yttria - stabilized ZrO2 buffer layers for YBCO coated conductors
Feng Xiao , Xiong Jie , Zhang Fei , Xia Yudong , Zhao Xiaohui , Tao Bowan. The influences of rapid growth of yttria - stabilized ZrO2 buffer layers for YBCO coated conductors[J]. Cryogenics and Superconductivity, 2012, 2(2): 19-23,33. DOI: 10.3969/j.issn.1001-7100.2012.02.005
Authors:Feng Xiao    Xiong Jie    Zhang Fei    Xia Yudong    Zhao Xiaohui    Tao Bowan
Affiliation:(State Key Laboratory of Electronic Thin Films and Integrated Devices,University of Electronic Science and Technology of China,Chengdu 610054,China)
Abstract:Direct current(dc) reactive sputtering is one of the most promising approaches for fabricating yttria-stabilized ZrO2(YSZ) buffer layers.In this paper,YSZ films were deposited on Y2O3-buffered Ni 5at.%W substrates with Zr target embedded with yttrium discs.The influences of the growth temperature and rolling speed were investigated detailedly.X-ray diffraction(XRD) measurement revealed that the YSZ films were preferential(002) orientation at 700℃.Atomic force microscopy(AFM) analysis indicated that the surface was smooth with few pores and crack free.The films prepared with different rolling speed were all c-axis oriented,however,their RMS and grain size were different.Rapid growth could restrain the oxidation of the substrates surface,improve the textures and enhance the fabricating efficiency.
Keywords:DC reactive sputtering  YSZ buffer layers  Rapid growth  Growth temperature  Rolling speed
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