Synthesis and reactivity of [18F]-N-fluorobenzenesulfonimide |
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Authors: | Teare Harriet Robins Edward G Arstad Erik Luthra Sajinder K Gouverneur Véronique |
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Institution: | Chemistry Research Laboratory, University of Oxford, 12 Mansfield Road, Oxford, UK OX1 3TA. |
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Abstract: | A novel 18F]NF reagent and two novel radiochemical transformations have been developed: 18F]NFSi has been prepared from sodium dibenzenesulfonimide and reacted in the presence of silyl enol ethers and allylsilanes to deliver labelled fluorinated ketones and allylic fluorides respectively; the radiosynthesis of the fluorinated A ring of vitamin D3 has also been completed with success. |
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