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| 液相色谱质谱联用检测血液和尿液中的 琥珀胆碱及对标样的稳定性评价 | |
| 引用本文： | 宣宇,孙楠,傅得锋,郑一平,徐晟捷. 液相色谱质谱联用检测血液和尿液中的 琥珀胆碱及对标样的稳定性评价[J]. 分析试验室, 2011, 30(8): 112-114 |
| 作者姓名： | 宣宇 孙楠 傅得锋 郑一平 徐晟捷 |
| 作者单位： | 1. 浙江工业大学化学工程与材料学院,杭州310014;浙江省公安物证鉴定中心,杭州310009 2. 浙江工业大学化学工程与材料学院,杭州,310014 3. 浙江省公安物证鉴定中心,杭州,310009 |
| 摘 要： | 采用OasisR WCX固相萃取柱,用50％甲醇溶液洗脱杂质,并用1 mL甲酸-乙腈-水(1:8:1)溶液进行淋洗目标物.采用LC/MS/ESI检测其母离子为145.1,并选择115.5作为其定量离子.在尿液和血液中进行了回收率实验,测得其定量检测限分别为0.92ng/mL,1.89ng/mL( 10倍S/N),方法的... |
| 关 键 词： | 琥珀胆碱 液相色谱质谱 尿液 血液 稳定性评价 |
Determination of succinycholine in the urine and plasma by LC/MS and stability evaluation of the reference materials |
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| XUAN Yu,SUN Nan,FU De-feng,ZHENG Yi-ping,XU Sheng-jie. Determination of succinycholine in the urine and plasma by LC/MS and stability evaluation of the reference materials[J]. Chinese Journal of Analysis Laboratory, 2011, 30(8): 112-114 | |
| Authors: | XUAN Yu SUN Nan FU De-feng ZHENG Yi-ping XU Sheng-jie |
| Affiliation: | XUAN Yu1,2,SUN Nan1,FU De-feng2,ZHENG Yi-ping2 and XU Sheng-jie2(1.College of Chemical Engineering and Materials,Zhejiang University of Technology,Hangzhou 310014,2.The Forensic Science Institute of Public Security of Zhejiang Province,Hangzhou 310009) |
| Abstract: | |
| Keywords: | Succinycholine High performance liquid chromatography electrospray ionization tandem mass spectrometry Urine Plasma Stability evaluation |
| 本文献已被 CNKI 万方数据 等数据库收录！ | |