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| 气相色谱-串联质谱法同时测定化妆品中的10种挥发性亚硝胺 | |
| 引用本文： | 马强,席海为,王超,白桦,席广成,苏宁,徐丽艳,王军兵. 气相色谱-串联质谱法同时测定化妆品中的10种挥发性亚硝胺[J]. 分析化学, 2011, 39(8): 1201-1207. DOI: 10.3724/SP.J.1096.2011.01201 |
| 作者姓名： | 马强 席海为 王超 白桦 席广成 苏宁 徐丽艳 王军兵 |
| 作者单位： | 1. 中国检验检疫科学研究院,北京,100123 2. 国家质量监督检验检疫总局进出口食品安全局,北京,100088 |
| 基金项目： | 质检公益性行业科研专项计划资助项目(No.200910267); 国家标准委员会计划资助项目(No.20090915-T-607); 中国检验检测疫科学研究院基本科研业务专项基金(No.2009JK016)资助 |
| 摘 要： | 建立了同时测定化妆品中10种挥发性亚硝胺(N-亚硝基二甲基胺,N-亚硝基二乙基胺、N-亚硝基二正丙基胺、N-亚硝基吗啉、N-亚硝基毗咯烷、N-亚硝基哌啶,N-亚硝基二正丁基胺、N-亚硝基二苯基胺、N-亚硝基二环己基胺及N-亚硝基二苄基胺)的气相色谱-串联质谱分析方法.膏霜、水剂、散粉、香波、唇膏等不同类型的化妆品样品分... |
| 关 键 词： | 固相萃取 气相色谱-串联质谱 化妆品 挥发性亚硝胺 |
Determination of 10 Volatile Nitrosamines in Cosmetics by Gas Chromatography-Tandem Mass Spectrometry |
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| MA Qiang,XI Hai-Wei,WANG Chao,BAI Hua,XI Guang-Cheng,SU Ning,XU Li-Yan,WANG Jun-Bing. Determination of 10 Volatile Nitrosamines in Cosmetics by Gas Chromatography-Tandem Mass Spectrometry[J]. Chinese Journal of Analytical Chemistry, 2011, 39(8): 1201-1207. DOI: 10.3724/SP.J.1096.2011.01201 | |
| Authors: | MA Qiang XI Hai-Wei WANG Chao BAI Hua XI Guang-Cheng SU Ning XU Li-Yan WANG Jun-Bing |
| Affiliation: | MA Qiang*1,XI Hai-Wei1,WANG Chao1,BAI Hua1,XI Guang-Cheng1,SU Ning1,XU Li-Yan2,WANG Jun-Bing1 1(Chinese Academy of Inspection and Quarantine,Beijing 100123) 2(Bureau of Import and Export Food Safety,General Administration of Quality Supervision,Inspection and Quarantine,Beijing 100088) |
| Abstract: | A comprehensive analytical method based on gas chromatography tandem mass spectrometry has been developed for the determination of 10 volatile nitrosamines(N-nitrosodimethylamine,N-nitrosodiethylamine,N-nitrosodi-n-propylamine,N-nitrosomorpholine,N-nitrosopyrrolidine,N-nitrosopiperidine,N-nitrosodi-n-butylamine,N-nitrosodiphenylamine,N-nitrosodicyclohexylamine and N-nitrosodibenzylamine) in cosmetics.Various cosmetic samples,including cream,lotion,powder,shampoo and lipstick,were extracted with appropriate ... |
| Keywords: | Solid phase extraction Gas chromatography-tandem mass spectrometry Cosmetics Volatile nitrosamines |
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