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一步法水热合成TiO2纳米线及其光催化性能
引用本文:韦秋芳,陈拥军.一步法水热合成TiO2纳米线及其光催化性能[J].高等学校化学学报,2011,32(11):2483-2489.
作者姓名:韦秋芳  陈拥军
作者单位:广西大学化学化工学院,南宁,530004
基金项目:国家自然科学基金(批准号:50862001); 广西大学人才引进基金资助
摘    要:以钛酸丁酯和异丙醇为原料,采用一步法在NaOH溶液中水解后直接进行水热反应,经焙烧处理,得到TiO2纳米线.采用扫描电子显微镜(SEM)、X射线衍射(XRD)和能谱分析(EDX)对产物进行了形貌、结构及成分的表征.考察了不同水热温度、碱液浓度、水热反应时间及焙烧温度等因素对产物的影响.结果表明,获得较好形貌TiO2纳米...

关 键 词:TiO2纳米线  钛酸丁酯  水热法  光催化活性
收稿时间:2011-02-28

One-step Hydrothermal Synthesis of TiO_2 Nanowires and Their Photocatalytic Activities
WEI Qiu-Fang,CHEN Yong-Jun.One-step Hydrothermal Synthesis of TiO_2 Nanowires and Their Photocatalytic Activities[J].Chemical Research In Chinese Universities,2011,32(11):2483-2489.
Authors:WEI Qiu-Fang  CHEN Yong-Jun
Institution:WEI Qiu-Fang,CHEN Yong-Jun (School of Chemistry and Chemical Engineering,Guangxi University,Nanning 530004,China)
Abstract:Titanium dioxide(TiO2) nanowires were synthesized by one-step hydrothermal method using tetrabutyl titanate,isopropanol and sodium hydroxide as starting materials.The synthesized TiO2 nanowires were characterized by scanning electron microscopy(SEM),X-ray diffraction(XRD) and energy dispersive X-ray spectrometry(EDX).The effects of reaction temperature,concentration of sodium hydroxide and reaction time on the formation of the nanowires were investigated.It is found that the optimum reaction temperature,con...
Keywords:TiO2 nanowire  Tetra-butyl titanate  Hydrothermal method  Photocatalytic activity  
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