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Solid phase carbon-13 NMR studies of dicyclohexyl-18-crown-6 ethers and some alkali metal phenoxide complexes
Affiliation:1. Key Laboratory of Computational Chemistry Based Natural Antitumor Drug Research & Development, Liaoning Province, School of Traditional Chinese Materia Medica, Shenyang Pharmaceutical University, Shenyang, 110016, People’s Republic of China;2. Department of Cardiology, Third Affiliated Hospital of Guangzhou Medical University, Guangzhou, 510150, China;3. Department of Virology II, National Institute of Infectious Diseases, 162-8640, Tokyo, Japan;4. Key Laboratory of Structure-Based Drug Design and Discovery, Ministry of Education, Shenyang Pharmaceutical University, Shenyang, 110016, China;1. School of Pharmacy, Faculty of Medicine, The Chinese University of Hong Kong, Hong Kong Special Administrative Region;2. School of Biomedical Sciences, Faculty of Medicine, The Chinese University of Hong Kong, Hong Kong Special Administrative Region;3. Joint Research Laboratory of Promoting Globalization of Traditional Chinese Medicines between The Chinese University of Hong Kong and Shanghai Institute of Materia Medica, Chinese Academy of Sciences, PR China;4. State Key Laboratory of Drug Research and Natural Products Chemistry Department, Shanghai Institute of Materia Medica, Chinese Academy of Sciences, Shanghai, PR China;5. Department of Pharmaceutical Biology, Johannes Gutenberg University, Mainz, Germany;1. Nikolaev Institute of Inorganic Chemistry, The Siberian Branch of the Russian Academy of Sciences, Av. Lavrentyev 3, Novosibirsk, 630090, Russian Federation;2. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, Leninskii pr. 31-4, Moscow, 119071, Russian Federation;3. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 119991, Russian Federation
Abstract:From C-13 CPMAS spectra, the asymmetric units in the crystalline state of a number of title species have been determined. Results are compared with available x-ray data and liquid phase C-13 spectra.
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