An efficient synthesis of [1,1]ferrocenophane via 1,1′-bis(6-fulvenyl)ferrocene |
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| Authors: | U.T. Mueller-Westerhoff A. Nazzal W. Prössdorf |
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| Affiliation: | IBM Research Laboratory, San Jose, California 95193 U.S.A. |
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| Abstract: | [1,1]Ferrocenophane can be prepared by reduction of 1,1′-bis(6-fulvenyl)ferrocene with complex borohydrides to give the dianion of 1,1′-bis(cyclopentadienylmethyl)ferrocene. Reaction of this dianion with ferrous chloride produces the ferrocenophane in good yield. |
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